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Beilstein J. Org. Chem. 2017, 13, 2869–2882, doi:10.3762/bjoc.13.279
Graphical Abstract
Figure 1: (a) Structures of isoleucine (1), leucine (2), and their fluorinated analogues 5,5,5-trifluoroisole...
Figure 2: Percentage of substrate remaining after incubation for 120 min (left) and 24 h (right) with α-chymo...
Figure 3: Cleavage positions observed in the digestion of library peptides with α-chymotrypsin.
Figure 4: Percentage of substrate remaining after incubation for 120 min (left) and 24 h (right) with pepsin ...
Figure 5: Cleavage positions for digestion of the different peptides with pepsin.
Figure 6: Percentage of substrate remaining after incubation for 120 min (left) and 24 h (right) with elastas...
Figure 7: Cleavage positions for digestion of the different peptides with elastase.
Figure 8: Percentage of substrate remaining after incubation for 120 min (left) and 24 h (right) with protein...
Figure 9: Cleavage positions found with proteinase K.
Figure 10: Dimension of stabilization or destabilization upon TfIle or HfLeu incorporation compared to the non...
Beilstein J. Org. Chem. 2013, 9, 2009–2014, doi:10.3762/bjoc.9.236
Scheme 1: Synthesis of optically active N-acyloxazolidinone 5 from 4,4,4-trifluorobutanoic acid. Conditions: ...
Scheme 2: Synthesis of enantiomerically pure (2S,3S)-5-F3Ile and (2R,3S)-5-F3-allo-Ile. TMGA = 1,1,3,3-tetram...
Figure 1: Retention times of Fmoc amino acids plotted against the van der Waals volume of their side chains. ...
Figure 2: CD spectra of K-5-F3Ile and K-Ile peptides (KX: Ac-YGGKAAAAKAXAAKAAAAK-NH2). The K-4’-F3Ile spectru...